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Re: [sdpd] Assistance
- To: "sdpd...@yahoogroups.com" <sdpd...@yahoogroups.com>
- Subject: Re: [sdpd] Assistance
- From: "Payzant, E. Andrew" <payzanta...@ornl.gov>
- Date: Fri, 23 Sep 2011 15:03:09 -0400
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- Thread-topic: [sdpd] Assistance
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<p>I believe that might be interpreted as "Read The Full Manual".
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Others might have a slightly different word to substitute for the "F".
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;-)
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Cheers,
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<br>
Andrew
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--
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E. Andrew Payzant
<br>
Senior R&D Staff Member
<br>
High Temperature Materials Laboratory
<br>
<br>
Oak Ridge National Laboratory
<br>
1 Bethel Valley Road
<br>
PO Box 2008, MS 6064
<br>
Building 4515, Room 113
<br>
Oak Ridge, TN, 37831-6064
<br>
<br>
ph: (865) 574-6538 FAX: (865) 574-3940
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web: <<a href="http://www.ms.ornl.gov/DTP/payzant.shtml";>http://www.ms.ornl.gov/DTP/payzant.shtml</a>>
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On 9/22/11 1:32 AM, "å¾?å??" <<a href="mailto:xujun16%40163.com";>xujun16...@163.com</a>> wrote:
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>What is RTFM?
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>
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>
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>
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>
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>
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>At 2011-09-22 13:24:49,"Lubomir Smrcok" <<a href="mailto:uachsmrk%40savba.sk";>uachsmrk...@savba.sk</a>> wrote:
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>>Or RTFM ...
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>>
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>>On Thu, 22 Sep 2011, wrote:
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>>
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>>>> They are about 100 nanometer?
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>>> in general, XRD can determine the crystal size in the range of
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>>>1nm-100nm. So you should check your data carefully under TEM or SEM, if
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>>>possible.
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>>>
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>>> There are several method to determine crystal size by XRD tech., The
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>>>Scherrer Equation, W-H, Fourier, and Rietveld. (see published journal -
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>>>crystal size determination round robin)
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>>>
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>>> Generally, two mehods W-H and Rietveld can be used in most software.
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>>>
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>>>> How to preceed data in specific software?
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>>> Maybe you should check the help file or E-mail Panalytical application
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>>>expert.
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>>>
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>>> Best,
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>>> Xu Jun
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>>>
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>>>
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>>>
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>>> At 2011-09-22 13:01:29,JB <<a href="mailto:javaedot2%40yahoo.com";>javaedot2...@yahoo.com</a>> wrote:
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>>>
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>>>
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>>> Thanks Wang, the particles are Calcite, probably rhombohedral, they
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>>>are about 100 nanometer, but I needed to know how to proceed with
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>>>X'pert HighScore Plus to determine the particle size after I have got
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>>>the XR diffraction patterns.
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>>>
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>>> Thanks in anticipation
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>>>
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>>> Make the world a better place to live in
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>>>
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>>> --- On Wed, 9/21/11, Xiaodong Wang <<a href="mailto:iangie%40126.com";>iangie...@126.com</a>> wrote:
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>>>
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>>> From: Xiaodong Wang <<a href="mailto:iangie%40126.com";>iangie...@126.com</a>>
<br>
>>> Subject: RE: [sdpd] Assistance
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>>> To:<a href="mailto:sdpd%40yahoogroups.com";>sdpd...@yahoogroups.com</a>
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>>> Date: Wednesday, September 21, 2011, 8:39 AM
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>>>
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>>>
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>>>
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>>> Is your particle calcite?
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>>>
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>>> Have you checked SEM images of these powder to see the extend of platy
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>>>shape?
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>>>
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>>> Just be careful about the preferred orientation effect when using
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>>>Bragg-Brentano geometry.
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>>>
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>>> If not, then you can use peak FWHM to estimate the coherent scatter
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>>>dimension.
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>>>
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>>> Yours Sincerely
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>>>
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>>> -------------------
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>>>
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>>> Xiaodong (Tony) Wang
<br>
>>>
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>>> Department of Imaging and Applied Physics
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>>>
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>>> Curtin University
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>>>
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>>>
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>>>From:<a href="mailto:sentto-1052548-2737-1316617777-iangie%3D126.com%40returns.groups.yahoo";>sentto-1052548-2737-1316617777-iangie=126.com...@returns.groups.yahoo</a>.
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>>>com
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>>>[mailto:<a href="mailto:sentto-1052548-2737-1316617777-iangie%3D126.com%40returns.groups.yah";>sentto-1052548-2737-1316617777-iangie=126.com...@returns.groups.yah</a>
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>>>oo.com] On Behalf Of JB
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>>>
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>>> Sent: 2011ÿÿ9ÿÿ21ÿÿ 23:10
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>>>
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>>> To:<a href="mailto:sdpd%40yahoogroups.com";>sdpd...@yahoogroups.com</a>
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>>>
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>>> Subject: [sdpd] Assistance
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>>>
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>>> Hello guys
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>>>
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>>> Can anyone help me, I need to calculate the particle size of a given
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>>>CaCO3 powder, how do I proceed (practically) using HighScore Plus. I
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>>>have the diffraction pattern.
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>>>
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>>> Thanks in anticipation.
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>>>
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>>> Make the world a better place to live in
<br>
>>>
<br>
>>> --- On Tue, 9/20/11, L_Solovyov <<a href="mailto:l_solovyov%40yahoo.com";>l_solovyov...@yahoo.com</a>
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>>><mailto:l_solovyov%40yahoo.com> > wrote:
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>>>
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>>> From: L_Solovyov <<a href="mailto:l_solovyov%40yahoo.com";>l_solovyov...@yahoo.com</a> <mailto:l_solovyov%40yahoo.com>
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>>>>
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>>>
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>>> Subject: [sdpd] Re: question
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>>>
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>>> To:<a href="mailto:sdpd%40yahoogroups.com";>sdpd...@yahoogroups.com</a> <mailto:sdpd%40yahoogroups.com>
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>>>
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>>> Date: Tuesday, September 20, 2011, 8:07 PM
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>>>
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>>>> What will be the real errors in this case?
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>>>
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>>> The uncertainties (sigmas) of the corrected profile intensities Icor
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>>>are:
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>>>
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>>> sigma(Icor) = sigma(Io)*Icor/Io = Icor/sqrt(Io)
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>>>
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>>> where Io is the observed uncorrected profile intensity.
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>>>
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>>> *******************************************************
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>>>
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>>> Leonid A. Solovyov
<br>
>>>
<br>
>>> Institute of Chemistry and Chemical Technology
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>>>
<br>
>>> 660049, K. Marx 42, Krasnoyarsk, Russia
<br>
>>>
<br>
>>> <a href="hxxp://sites.google.com/site/solovyovleonid">hxxp://sites.google.com/site/solovyovleonid</a>
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>>>
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>>> *******************************************************
<br>
>>>
<br>
>>> --- <a href="mailto:Insdpd%40yahoogroups.com";>Insdpd...@yahoogroups.com</a> <mailto:sdpd%40yahoogroups.com> , Radu
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>>>Baies <radu.baies...@...> wrote:
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>>>
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>>>>
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>>>
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>>>> Dear All,
<br>
>>>
<br>
>>>> Our diffractometer is running with a variable divergence slit. The
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>>>
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>>>> data can be corrected for this using HighScore program.
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>>>
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>>>> In FullProf the errors are calculated assuming a Poisson distribution.
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>>>
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>>>> What will be the real errors in this case?
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>>>
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>>>> Thanks
<br>
>>>
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>>>>
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>>>
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>>> [Non-text portions of this message have been removed]
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>>>
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>>> [Non-text portions of this message have been removed]
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>>>
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>>> [Non-text portions of this message have been removed]
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>>>
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>>>
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>>>
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>>>
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>>> [Non-text portions of this message have been removed]
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>>>
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>>>
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>>>
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>>> ------------------------------------
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>>>
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>>> Yahoo! Groups Links
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>>>
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>>>
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>>>
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>>>
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>>
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>>[Non-text portions of this message have been removed]
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>>
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>>
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>>
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>>------------------------------------
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>>
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>>Yahoo! Groups Links
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>>
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>>
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>>
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>
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>[Non-text portions of this message have been removed]
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>------------------------------------
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>
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>Yahoo! Groups Links
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font-weight: 700;
}
dd.last p span.yshortcuts {
margin-right: 0;
}
div.attach-table div div a {
text-decoration: none;
}
div.attach-table {
width: 400px;
}
div.file-title a, div.file-title a:active, div.file-title a:hover, div.file-title a:visited {
text-decoration: none;
}
div.photo-title a, div.photo-title a:active, div.photo-title a:hover, div.photo-title a:visited {
text-decoration: none;
}
div#ygrp-mlmsg #ygrp-msg p a span.yshortcuts {
font-family: Verdana;
font-size: 10px;
font-weight: normal;
}
.green {
color: #628c2a;
}
.MsoNormal {
margin: 0 0 0 0;
}
o {
font-size: 0;
}
#photos div {
float: left;
width: 72px;
}
#photos div div {
border: 1px solid #666666;
height: 62px;
overflow: hidden;
width: 62px;
}
#photos div label {
color: #666666;
font-size: 10px;
overflow: hidden;
text-align: center;
white-space: nowrap;
width: 64px;
}
#reco-category {
font-size: 77%;
}
#reco-desc {
font-size: 77%;
}
.replbq {
margin: 4px;
}
#ygrp-actbar div a:first-child {
/* border-right: 0px solid #000;*/
margin-right: 2px;
padding-right: 5px;
}
#ygrp-mlmsg {
font-size: 13px;
font-family: Arial, helvetica,clean, sans-serif;
*font-size: small;
*font: x-small;
}
#ygrp-mlmsg table {
font-size: inherit;
font: 100%;
}
#ygrp-mlmsg select, input, textarea {
font: 99% Arial, Helvetica, clean, sans-serif;
}
#ygrp-mlmsg pre, code {
font:115% monospace;
*font-size:100%;
}
#ygrp-mlmsg * {
line-height: 1.22em;
}
#ygrp-mlmsg #logo {
padding-bottom: 10px;
}
#ygrp-mlmsg a {
color: #1E66AE;
}
#ygrp-msg p a {
font-family: Verdana;
}
#ygrp-msg p#attach-count span {
color: #1E66AE;
font-weight: 700;
}
#ygrp-reco #reco-head {
color: #ff7900;
font-weight: 700;
}
#ygrp-reco {
margin-bottom: 20px;
padding: 0px;
}
#ygrp-sponsor #ov li a {
font-size: 130%;
text-decoration: none;
}
#ygrp-sponsor #ov li {
font-size: 77%;
list-style-type: square;
padding: 6px 0;
}
#ygrp-sponsor #ov ul {
margin: 0;
padding: 0 0 0 8px;
}
#ygrp-text {
font-family: Georgia;
}
#ygrp-text p {
margin: 0 0 1em 0;
}
#ygrp-text tt {
font-size: 120%;
}
#ygrp-vital ul li:last-child {
border-right: none !important;
}
-->
</style>
</head>
<!--~-|**|PrettyHtmlEnd|**|-~-->
</html>
<!-- end group email -->
</x-html>