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[sdpd] Re: Assistance



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      <p>&gt;The difficulty in such studies, when using a laboratory instrument,<br>
&gt;is to ensure that the reference material powder pattern is recorded with<br>
&gt;same conditions as the sample with size-strain effect, including<br>
&gt;the need for similar absorption, compaction.<br>
<br>
The HighScore Help gives a detailed description of the Size-Strain analysis procedure. It suggests using an external standard for the instrumental contribution determination. However, to minimize the potential problems of absorption, compaction, surface roughness etc., it is better to admix the standard powder to the sample studied.<br>
<br>
*******************************************************<br>
Leonid A. Solovyov<br>
Institute of Chemistry and Chemical Technology<br>
660049, K. Marx 42, Krasnoyarsk, Russia<br>
<a href="http://sites.google.com/site/solovyovleonid";>http://sites.google.com/site/solovyovleonid</a><br>
*******************************************************<br>
<br>
--- In <a href="mailto:sdpd%40yahoogroups.com";>sdpd...@yahoogroups.com</a>, Armel Le Bail &lt;xtal...@...&gt; wrote:<br>
&gt;<br>
&gt; <br>
&gt; &gt;I believe that might be interpreted as &quot;Read The Full Manual&quot;.<br>
&gt; &gt;<br>
&gt; &gt;Others might have a slightly different word to substitute for the &quot;F&quot;.<br>
&gt; &gt;<br>
&gt; &gt;;-)<br>
&gt; <br>
&gt; Sure, but the result is the same.<br>
&gt; <br>
&gt; Being not a Highscore user, I can't say, but probably there is<br>
&gt; some possibility described in the F. Manual to use the integral<br>
&gt; breadth relations to size/strain effects, taking account of the geometrical<br>
&gt; aberrations obtained from some reference material. The difficulty in<br>
&gt; such studies, when using a laboratory instrument, is to ensure<br>
&gt; that the reference material powder pattern is recorded with<br>
&gt; same conditions as the sample with size-strain effect, including<br>
&gt; the need for similar absorption, compaction.<br>
&gt; <br>
&gt; Best wishes,<br>
&gt; <br>
&gt; Armel<br>
&gt;<br>
<br>
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