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Fwd: [sdpd] Background
- To: sdpd...@yahoogroups.com
- Subject: Fwd: [sdpd] Background
- From: Peter Stephens <peter.stephens...@stonybrook.edu>
- Date: Mon, 29 Apr 2013 18:32:37 -0400
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<p>80 background coefficients does seem like an awfully large number. Are you<br>
unable to get a decent refinement with fewer (like, at most, ten)? Is it a<br>
particularly structured background?<br>
<br>
A general comment -- questions like that are very hard to give meaningful<br>
answers without knowing more. I think most of the people in this<br>
discussion group would not be comfortable giving serious advice without<br>
seeing the data, the structure, the refinement, etc. I know that we're not<br>
supposed to attach big files on this discussion group, and I'm sure you<br>
have concerns about not splashing your unfinished results on the web. I'll<br>
be willing to take, at least, a very brief look at it if you care to send<br>
me a screen shot of the refinement and maybe a bit of info about the<br>
compound, how the data were taken, etc. Start there, and I'll ask you if I<br>
need more data to consider. I pledge to hold any information you send me<br>
in confidence. If OK with you, send to <a href="mailto:peter.stephens%40stonybrook.edu";>peter.stephens...@stonybrook.edu</a><br>
<br>
Best,<br>
Peter<br>
<br>
On Mon, Apr 29, 2013 at 11:25 AM, sabrina belkhiri <<a href="mailto:belkhirisab%40yahoo.fr";>belkhirisab...@yahoo.fr</a>>wrote:<br>
<br>
> **<br>
><br>
><br>
> Dear SDPD groups,<br>
><br>
> I have a simple question :<br>
><br>
> During the refinement of my structure which contains 19 atomes among them<br>
> 6 heavy atomes, I refined 150 parameters, including 80 coefficients of the<br>
> background in order to get a good fitting. my question is :<br>
><br>
> Is it correct in the Rietveld refinement to use 80 coefficients of the<br>
> background ? because It seems to higher.<br>
><br>
> Thank you to answer me because I really need this answer, it's so<br>
> important for me.<br>
><br>
> [Non-text portions of this message have been removed]<br>
><br>
><br>
><br>
**************************<br>
Peter W. Stephens<br>
Professor, Department of Physics and Astronomy<br>
Associate Dean for Curriculum, College of Arts and Sciences<br>
Stony Brook University<br>
(631) 632-8156<br>
<a href="http://mini.physics.sunysb.edu/~pstephens";>http://mini.physics.sunysb.edu/~pstephens</a><br>
Please update your records to my new email: <a href="mailto:peter.stephens%40stonybrook.edu";>peter.stephens...@stonybrook.edu</a><br>
<br>
[Non-text portions of this message have been removed]<br>
<br>
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font-family: Verdana;
font-weight: 700;
}
dd.last p span.yshortcuts {
margin-right: 0;
}
div.attach-table div div a {
text-decoration: none;
}
div.attach-table {
width: 400px;
}
div.file-title a, div.file-title a:active, div.file-title a:hover, div.file-title a:visited {
text-decoration: none;
}
div.photo-title a, div.photo-title a:active, div.photo-title a:hover, div.photo-title a:visited {
text-decoration: none;
}
div#ygrp-mlmsg #ygrp-msg p a span.yshortcuts {
font-family: Verdana;
font-size: 10px;
font-weight: normal;
}
.green {
color: #628c2a;
}
.MsoNormal {
margin: 0 0 0 0;
}
o {
font-size: 0;
}
#photos div {
float: left;
width: 72px;
}
#photos div div {
border: 1px solid #666666;
height: 62px;
overflow: hidden;
width: 62px;
}
#photos div label {
color: #666666;
font-size: 10px;
overflow: hidden;
text-align: center;
white-space: nowrap;
width: 64px;
}
#reco-category {
font-size: 77%;
}
#reco-desc {
font-size: 77%;
}
.replbq {
margin: 4px;
}
#ygrp-actbar div a:first-child {
/* border-right: 0px solid #000;*/
margin-right: 2px;
padding-right: 5px;
}
#ygrp-mlmsg {
font-size: 13px;
font-family: Arial, helvetica,clean, sans-serif;
*font-size: small;
*font: x-small;
}
#ygrp-mlmsg table {
font-size: inherit;
font: 100%;
}
#ygrp-mlmsg select, input, textarea {
font: 99% Arial, Helvetica, clean, sans-serif;
}
#ygrp-mlmsg pre, code {
font:115% monospace;
*font-size:100%;
}
#ygrp-mlmsg * {
line-height: 1.22em;
}
#ygrp-mlmsg #logo {
padding-bottom: 10px;
}
#ygrp-msg p a {
font-family: Verdana;
}
#ygrp-msg p#attach-count span {
color: #1E66AE;
font-weight: 700;
}
#ygrp-reco #reco-head {
color: #ff7900;
font-weight: 700;
}
#ygrp-reco {
margin-bottom: 20px;
padding: 0px;
}
#ygrp-sponsor #ov li a {
font-size: 130%;
text-decoration: none;
}
#ygrp-sponsor #ov li {
font-size: 77%;
list-style-type: square;
padding: 6px 0;
}
#ygrp-sponsor #ov ul {
margin: 0;
padding: 0 0 0 8px;
}
#ygrp-text {
font-family: Georgia;
}
#ygrp-text p {
margin: 0 0 1em 0;
}
#ygrp-text tt {
font-size: 120%;
}
#ygrp-vital ul li:last-child {
border-right: none !important;
}
-->
</style>
</head>
<!--~-|**|PrettyHtmlEnd|**|-~-->
</html>
<!-- end group email -->
</x-html>