SHELXS86 with full data : 325 hkl
ATOM PEAK X Y Z SOF HEIGHT DISTANCES AND ANGLES
1 474. 0.3574 0.0424 0.8125 1.000 2.53 0 2 3.062
0 3 2.256 21.6
0 4 1.255 82.6 61.1
0 5 2.553 163.5 166.9 111.0
2 251. 0.0685 0.0465 0.5993 1.000 2.28 0 1 3.062
0 3 1.272 40.7
3 184. 0.1597 -0.1124 0.6541 1.000 2.58 0 1 2.256
0 2 1.272 117.7
0 4 1.983 33.7 151.1
4 178. 0.3444 -0.1921 0.7556 1.000 2.95 0 1 1.255
0 3 1.983 85.2
5 174. 0.5801 0.1434 1.1160 1.000 2.14 0 1 2.553
SHELXS86 with partial data : 286 hkl
ATOM PEAK X Y Z SOF HEIGHT DISTANCES AND ANGLES
1 478. 0.7154 0.0534 0.7165 1.000 3.08 0 2 3.088
0 3 1.581 165.5
0 4 1.274 46.7 131.6
0 5 2.926 123.6 46.1 89.1
2 344. 1.0000 0.0000 1.0000 0.500 3.65 0 1 3.088
0 4 2.401 22.7
3 244. 0.5635 0.0597 0.6788 1.000 3.10 0 1 1.581
0 4 2.607 21.4
0 5 2.155 102.0 82.9
4 242. 0.7948 -0.1307 0.7212 1.000 2.69 0 1 1.274
0 2 2.401 110.6
0 3 2.607 27.0 135.5
5 142. 0.5142 -0.3034 0.9168 1.000 3.27 0 1 2.926
0 3 2.155 31.9
SHELXS86 with partial data : 242 hkl
ATOM PEAK X Y Z SOF HEIGHT DISTANCES AND ANGLES
1 561. 0.3571 0.0546 0.8101 1.000 3.48 0 2 2.421
0 3 2.965 24.6
0 4 2.279 97.5 116.4
0 5 1.300 26.2 24.1 94.1
2 307. 0.1487 -0.1356 0.6612 1.000 3.94 0 1 2.421
0 3 1.265 102.6
0 5 1.379 24.6 89.1
3 274. 0.0760 0.0565 0.6242 1.000 3.41 0 1 2.965
0 2 1.265 52.8
0 5 1.857 16.6 48.0
4 240. 0.4316 -0.2415 1.2448 1.000 3.07 0 1 2.279
0 5 2.703 28.7
5 154. 0.2370 0.0117 0.8701 1.000 3.14 0 1 1.300
0 2 1.379 129.3
0 3 1.857 139.3 42.9
0 4 2.703 57.2 116.1 157.1