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Re: [sdpd] calibration problems with Silicon+gsas
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<p>Dear Lujun,<br>
<br>
I apologize if I did not let attention enough about your recording <br>
conditions (not yet had a look to your raw data):<br>
1°) Your work with a STADI-P with a linear PSD ? Could you please let us <br>
know its counting aperture ?<br>
2°) What is your sample configuration: capillary (diameter ?) classical <br>
Debye-Scherrer or transmission between two milar foils ?<br>
<br>
By having a look on your background details, as Pr. Reinhard Kleeberg <br>
already told you: it shows strange periodical oscillations.<br>
My question is: what is your PSD step size ? 0.5° 2theta ?<br>
<br>
Could it please be possible to know a little more on your PSD <br>
calibration file ? Do you have an access to the *.cal and *.lcl files ?<br>
Of course, I mean your current calibration files (those ware used for <br>
you Silicon data collection).<br>
<br>
Thank you for you informations<br>
<br>
Best,<br>
<br>
JM<br>
____________<wbr>_________<wbr>_________<wbr>_________<wbr>____<br>
<br>
Dr. Jean-Marc LE MEINS<br>
Ecole Nationale Supérieure de Chimie<br>
LMPC - UMR CNRS 7016<br>
3 rue Alfred Werner<br>
F-68093 Mulhouse CEDEX<br>
<br>
Tel: +33 (0)3 89 33 68 82<br>
FAX: +33 (0)3 89 33 68 85<br>
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<br>
[Non-text portions of this message have been removed]<br>
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