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R: [sdpd] XRD intensity



Dear Hysen,
I'm just a PhD student, and so I'm not so expert about this problem. But the
only thing that comes in my mind (probably you have already tried it...,
excuse me!!)  is to improve the counting times maybe to 8 Seconds, and to
use a larger receviving slit.
Bye,
marco

----- Original Message -----
From: Hysen Thomas <colloid_h...@yahoo.co.uk>
To: <sdpd...@yahoogroups.com>
Sent: Friday, March 11, 2005 4:21 AM
Subject: [sdpd] XRD intensity


>
>
> Dear all
> I am hysen from cochin university ,Kerala. I am working on
> nanomagnetic materials. specifically an alloy of irom molybdenum boron
> and nickel. I have prepared thin films of this having thickness around
> 30 nm by resistive heating and annealed the sample upto the
> crystallization temperature of the bulk. But interestingly the xrd
> spectrum shows peaks which are very feeble which has intensity
> comparable to that of the noise. Can anybody has any suggestionsto
> improve the xrd spectrum. Due to this low intensity i cant do any fitting.
> Thank you in advance
> Hysen Thomas researcher
> Cusat
> Cochin 22
> Kerala
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> Yahoo! Groups Links
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