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Re: [sdpd] XRD intensity
Hysen
what is your diffractometer configuration ? Take care of fluorescence
arising from Fe in case of using for instance CuKa1 with a incident-beam
monochromator. Have you tried with a graphite monoch. behind your sample ?
Thierry
At 03:21 11/03/2005 +0000, vous avez écrit:
>Dear all
>I am hysen from cochin university ,Kerala. I am working on
>nanomagnetic materials. specifically an alloy of irom molybdenum boron
>and nickel. I have prepared thin films of this having thickness around
>30 nm by resistive heating and annealed the sample upto the
>crystallization temperature of the bulk. But interestingly the xrd
>spectrum shows peaks which are very feeble which has intensity
>comparable to that of the noise. Can anybody has any suggestionsto
>improve the xrd spectrum. Due to this low intensity i cant do any fitting.
>Thank you in advance
>Hysen Thomas researcher
>Cusat
>Cochin 22
>Kerala
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>Yahoo! Groups Links
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Thierry Bataille
LCSIM UMR CNRS 6511
Cristallographie des Poudres et Réactivité des Solides
Institut de Chimie de Rennes
Université de RENNES I
Avenue du Général Leclerc
F-35042 RENNES cedex, France
Tel. (+33) 2 23 23 58 05 Fax. (+33) 2 23 23 68 40
mailto:Thierry.Bataille...@univ-rennes1.fr
http://perso.univ-rennes1.fr/thierry.bataille
http://www.lcsim.univ-rennes1.fr
http://www.chimie.univ-rennes1.fr
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